New Products
Find 2 4 6-Tribromophenol CAS 118-79-6, CAS NO 118-79-6, Others Name Of BROMOL on Industry Directory, Reliable Manufacturer/Supplier/Factory from China.
Payment Type: | L/C,T/T,Money Gram,Western Union |
---|---|
Incoterm: | FOB,CIF |
Min. Order: | 1 Kilogram |
Delivery Time: | 3 Days |
Model No.: CAS NO 118-79-6
Free sample 2 4 6-Tribromophenol CAS 118-79-6
Tribromophenol (2,4,6-Tribromophenol; Abbreviation: TBP) is an aromatic compound. White acicular or prismatic crystals with a pungent odor.
production method
1. Add phenol to the reaction kettle, stir and add water and heat up to 60°C. Add bromine dropwise. Continue stirring for 30 minutes after the addition is complete. Then it was cooled to 40°C and filtered. The cake was washed with water until neutral to obtain crude product. The crude product was dissolved in ethanol at 70° C., activated carbon was added for decoloration, and after filtering, an equal amount of water was mixed with the filtrate, ie, needle-like crystals were precipitated as a finished product. The yield is about 96%.
2. The following three routes are used to produce tribromophenol.
(1) Direct bromination method (phenol-bromine water oxidation method) At present, domestic use of the traditional process --- using the bromine water oxidation and substitution of the dual characteristics, and phenol reaction, generate white tribromophenol precipitation. The process is as follows. 1 Preparation Dissolve phenol in water and slowly add the equivalent of bromine water (KBr as cosolvent) under stirring. Control the temperature at 60 °C. Add dropwise, reaction for 30 min, cool to 40 °C, filter. The solution was washed with dilute aqueous sodium bisulfite, washed with water until neutral, and dried to give crude 2,4,6-tribromophenol. 2 Refinement The above crude crystals are dissolved in hot anhydrous ethanol, decolorized by adding activated carbon, filtered, and then the same amount of water is mixed with the filtrate, ie, needle-like crystal products are precipitated, and the yield is 96%. 3 Hydrogen bromide recovery 0.2 mol of benzene was dissolved in water and 0.3 mol of bromine water was added dropwise with vigorous stirring. After the addition was completed, 0.3 mol of chlorine gas was slowly fed. After the reaction was complete, the mixture was filtered and washed with dilute aqueous sodium bisulfite solution. And then washed with water to neutral, dried product. ...
use
It is used as reactive flame retardant and is suitable for adhesives and sealants such as epoxy Resin, polyurethane, polycarbon grease, and phenolic resin. It can also be used as a fungicide.
Why Choose Us?
1. Quality Price
We are the manufacturer, so we can provide the competitive price and high quality product.
2. Packing
Products could be packaged according to customer's specializedrequirements.
3. Transport
The products can be transported by Courier, by Air or by Sea.
4. Service
We offer specialized logistic service including export declaration,customs clearance and every detail during shipment. This makes us able to offer you one-stop service from the order to the products transported to your hand.
Product expansion
Contact us if you need more details on 2 4 6-Tribromophenol CAS 118-79-6. We are ready to answer your questions on packaging, logistics, certification or any other aspects about CAS NO 118-79-6、Others Name of BROMOL. If these products fail to match your need, please contact us and we would like to provide relevant information.Product Categories : Catalysts And Auxiliaries